The bulletin of the Yamaguchi Medical School

Continued by:Medical Science & Innovation
EISSN:2758-5441

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The bulletin of the Yamaguchi Medical School Volume 6 Issue 3
published_at 1959-04-30

ON THE MECHANISM OF FLORENCE’S CRYSTAL FORMATION : Ⅰ. PREPARATION OF NEURINE CHLORIDE

ON THE MECHANISM OF FLORENCE’S CRYSTAL FORMATION : Ⅰ. PREPARATION OF NEURINE CHLORIDE
Takemoto Kazushige
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Descriptions
Neurine chloride could be prepared by dehydrochlorination of chlorocholine chloride synthesized by the interaction of ethylene chloride and trimethylamine. It was a tetragonal prism or pyramid, reacting with Florence's reagent to give microscopic rectangular crystals which could not be distinguished from typical Florence's crystal. The infra-red spectrum of neurine chloride was briefly discussed.