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フルテキストURLA020017000301.pdf ( 1.3MB ) 公開日 2010-04-16
タイトルOn the Separation and Identification of Sulfonamides by the Thin-Layer Chromatography and the Detection of Sulfa Drug in the Cadaveric Blood
作成者Furuno, Junji
Sugawara, Norisuke
Kan, Takeshi
作成者ヨミフルノ, ジュンジ
スガワラ, ノリスケ
カン, タケシ
作成者所属山口大学医学部
内容記述(抄録等)The autors have described the separation and identification of seven kinds of sulfonamides by means of the thin-layer chromatograghy and an example for the detection of sulfamonomethoxine sodium in the cadaveric blood. In the separation of these sulfonamides, the developers of chloroform-methanol system which consist of two or more kinds of polar and non-polar solvents, gave the satisfactory result. All these sulfonamides could be detected even in a very small quantities of 0.1 μg by using p-dimethylaminobenzaldehyde or diazo reagent and the color was very clear. As a result, both reagents would be expected to be available for the detecting reagent in the usual analysis of sulfonamides. From the blood (8 ml) of a man aged 52 who ”Daimeton” injection was intravenously received and suddenly died, sulfamonomethoxine sodium was separated and identified through the analysis coupled with the thin-layer chromatography and ultraviolet absorption spectrophotometry. The quantities of sulfamonomethoxine sodium determined about the remainder of blood extract after the qualititive analysis was approximately 3.0 mg.
本文言語eng
主題医学
資料タイプtext
ファイル形式application/pdf
出版者Yamaguchi University Graduate School of Medicine
NII資料タイプ紀要論文
ISSN0513-1812
NCIDAA00594272
学内刊行物(紀要等)The bulletin of the Yamaguchi Medical School
掲載誌名The bulletin of the Yamaguchi Medical School
掲載誌名別表記山口医科大学紀要
17
3-4
開始ページ179
終了ページ189
発行日1970-12
著者版/出版社版出版社版
リポジトリIDA020017000301
地域区分山口大学
URIhttp://www.lib.yamaguchi-u.ac.jp/yunoca/handle/A020017000301